A saponification-triggered gelation of ester-based Zn(II) complex through conformational transformations.

نویسندگان

  • Ashish Kumar
  • Mrigendra Dubey
  • Amit Kumar
  • Daya Shankar Pandey
چکیده

Novel saponification-triggered gelation in an ester-based bis-salen Zn(II) complex (1) is described. Strategic structural modifications induced by NaOH in 1 tune the dipolar-/π-interactions leading to J-aggregation and the creation of an inorganic gel material (IGM), which has been established by photophysical, DFT and rheological studies.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Homochiral coordination polymeric gel: Zn(2+)-induced conformational changes leading to J-aggregated helical fibres formation.

A novel chiral coordination polymeric gel based on an amino acid derived symmetrical ligand, specific base, and Zn(2+) has been described. Zn(2+) induced conformational reorganization in the ligand leads to gelation via J-aggregated helical fibres. The vital role played by π-π stacking in gelation has been monitored by fluorescence and NMR spectroscopy.

متن کامل

Comparing a mononuclear Zn(II) complex with hydrogen bond donors with a dinuclear Zn(II) complex for catalysing phosphate ester cleavage.

Introducing ligand based hydrogen bond donors to increase the activity of a mononuclear Zn(II) complex for catalysing phosphate ester cleavage can be a more effective strategy than making the dinuclear analogue.

متن کامل

Evaluation of Methyl Ester Production Using Cement as a Heterogeneous Catalyst

This experiment is an investigation of used cooking oil as a sustainable and renewable resource for methyl ester production. with more than 95.5% production yield, thermally activated hydrated cement has been carefully discussed as a catalyst in the transesterification of used cooking oil into methyl ester to use waste cement as a heterogeneous catalyst for methyl ester production through elect...

متن کامل

Biophysical and Molecular Docking Studies of Human Serum Albumin Interactions with a Potential Anticancer Pt(II) Complex

The interaction between [Pt(phen)(pyrr-dtc)]NO3 (where phen = 1,10-phenanthroline and pyrr-dtc =pyrrolidinedithiocarbamat) with human serum albumin (HSA) was studied by fluorescence, UV–vis absorption, circular dichroism (CD) spectroscopy and molecular docking technique under like physiological condition in Tris–HCl buffer solution at pH 7.4. UV-Vis absorption spectroscopy indicates that the pro...

متن کامل

Light-triggered Supramolecular Isomerism in a Self-catenated Zn(II)-organic Framework: Dynamic Photo-switching CO2 Uptake and Detection of Nitroaromatics

A self-catenated Zn(II)-organic framework formulated as [Zn2(3,3'-bpeab)(oba)2]·DMF (1) exhibiting a six-connected 44·610·8 topology has been successfully synthesized through the mixed-ligand of kinked 3,3'-bis[2-(4-pyridyl)ethenyl]azobenzene (3,3'-bpeab) and 4,4'-oxybis-benzoic acid (H2oba) under solvothermal condition. UV light triggers isomerization of complex 1 in a single-crystal-to-single...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Chemical communications

دوره 50 70  شماره 

صفحات  -

تاریخ انتشار 2014